HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Benzyl methyl(piperidin-4-yl)carbamate hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Carbamic acid, (1-acetyl-4-piperidinyl)methyl-, phenylmethyl ester | HCID 19761266 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Benzyl methyl(piperidin-4-yl)carbamate hydrochloride | HCID 18677745 | — |
Reaction Steps
14.5 g of the compound obtained in Stage B are refluxed with 50 ml of methanol and 30 ml of 6N hydrochloride acid for 20 hours. After evaporation the hydrochloride of the desired product is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05189045 |
| Source dataset | uspto-grants-1993_02 |
| ORD ID | ord-3af9414327cd40cba4050025774f8226 |
| Source note | uspto-grants-1993_02 |