HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl 2-isobutyl-3-(methoxycarbonyl)-propionate → HCID 10583768, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl 2-isobutyl-3-(methoxycarbonyl)-propionate | HCID 15408557 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 10583768 | HCID 10583768 | 86.1% |
Reaction Steps
A mixture of 8.01 g (0.029 mol) of (2) and 1 g of 10% palladium on carbon in 50 mL of methanol was hydrogenated at room temperature under 4 atmospheres of hydrogen gas for 8 hr. After removal of the catalyst by filtration the filtrate was evaporated to dryness under reduced pressure to give 4.7 g (86% yield) of 2-isobutyl-3-(methoxycarbonyl)-propionic acid (3) as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05189178 |
| Source dataset | uspto-grants-1993_02 |
| ORD ID | ord-c98fe65d5a3e43aa9818c7a13fbdc35a |
| Source note | uspto-grants-1993_02 |