Thionyl Chloride → HCID 20359910, compound

HRID 2082635Notes

Reaction equation

HRID 2082635 reaction equation
[CH3:1][CH:2]([CH2:22][CH3:23])[CH2:3][C:4]1[CH:21]=[CH:20][C:7]([C:8]([O:10][C:11]2[CH:19]=[CH:18][C:14]([C:15](O)=[O:16])=[CH:13][CH:12]=2)=[O:9])=[CH:6][CH:5]=1.S(Cl)([Cl:26])=O>>[CH3:1][CH:2]([CH2:22][CH3:23])[CH2:3][C:4]1[CH:21]=[CH:20][C:7]([C:8]([O:10][C:11]2[CH:19]=[CH:18][C:14]([C:15]([Cl:26])=[O:16])=[CH:13][CH:12]=2)=[O:9])=[CH:6][CH:5]=1

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 20359906HCID 20359906, compound

Product 1

HCID 20359910HCID 20359910, compound

Procedure

A mixture of (+)-4-(4'-β-methylbutylbenzoyloxy)-benzoic acid (5.7g, 0.0182m) and thionyl chloride (20ml) was refluxed for four hours. The excess thionyl chloride was distilled and the residue was used in the following reaction without purification.

Workup

  1. temperaturewas refluxed for four hours
  2. distillationThe excess thionyl chloride was distilled
  3. customthe residue was used in the following reaction without purification

Sources & evidence

ORD record
ord-2974ca04dbf345448341b9d73d5e0e23
Source dataset
uspto-grants-1978_04
Patent number
US04082428

Reaction notes

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