Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Chlorine | HCID 24526 | — |
| Reactant | HCID 66687793 | HCID 66687793 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | N-Chlorophthalimide | HCID 18997 | 90% |
Reaction Steps
To 170 ml. of methylene chloride saturated with chlorine and maintained at 0° C. were added 8.3 grams (49 mmoles) of sodium phthalimide. The resulting mixture was warmed to 20° C. and was stirred for 1.5 hours. The resulting precipitated sodium chloride was removed by filtration, and the filtrate was evaporated to dryness to afford 8.0 grams (90% yield) of N-chlorophthalimide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04082766 |
|---|
| Source dataset | uspto-grants-1978_04 |
|---|
| ORD ID | ord-73ca27420e2345cb84c35bdca3775fe5 |
|---|
| Source note | uspto-grants-1978_04 |
|---|
