Nitric Acid → HCID 19989839, compound

HRID 2082821Notes

Reaction equation

HRID 2082821 reaction equation
[Br:1][C:2]1[CH:14]=[CH:13][C:5]([C:6]([CH2:8][CH2:9][C:10]([OH:12])=[O:11])=[O:7])=[CH:4][CH:3]=1.[N+:15]([O-])([OH:17])=[O:16]>>[Br:1][C:2]1[CH:3]=[CH:4][C:5]([C:6]([CH2:8][CH2:9][C:10]([OH:12])=[O:11])=[O:7])=[CH:13][C:14]=1[N+:15]([O-:17])=[O:16]

Participants

3

Reactant 2

HCID 944Nitric AcidHCID 806463-(4-Bromobenzoyl)propionic acid

Product 1

HCID 19989839HCID 19989839, compound

Procedure

3-(4-Bromobenzoyl)propionic acid was added in portions to well stirred fuming nitric acid at -15° C and the resultant mixture stirred a further 30 minutes then poured into ice-water to give 3-(4-bromo-3-nitrobenzoyl)propionic acid.

Sources & evidence

ORD record
ord-011aeec2e6344073a74cd5797a1d8c77
Source dataset
uspto-grants-1978_04
Patent number
US04082843

Reaction notes

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