Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1,7-Octadiene | HCID 19460 | — |
| Reactant | Trichlorosilane | HCID 24811 | — |
| Product | 7-Octenyltrichlorosilane | HCID 104122 | — |
| Product | Octane-1,8-diylbis[trichlorosilane] | HCID 104123 | — |
Reaction Steps
In another experiment, 220 g (1.62 mole) trichlorosilane was added slowly in 20 minutes to a stirred mixture of 660 g (6 mole) 1,7-octadiene at 35° C. Subsequently, the reaction mixture was heated at 50° C for 24 hours to complete the addition and then fractionally distilled. This resulted in 322 g, i.e., 82%, 7-octenyl trichlorosilane and 24 g, i.e., 12%, 1,8-bis-trichlorosilyl octane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04083803 |
|---|
| Source dataset | uspto-grants-1978_04 |
|---|
| ORD ID | ord-6d9e664e8ec74618bb087c04ea030103 |
|---|
| Source note | uspto-grants-1978_04 |
|---|
