HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidine → HCID 70623472, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | HCID 20358952 | HCID 20358952 | — |
| Reactant | HCID 54067553 | HCID 54067553 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 70623472 | HCID 70623472 | 37.8% |
Reaction Steps
A solution of 4.18 g (0.01 mol) of crude 2-(α-chloroacetylaminobenzyl)-5-(3-methyl-2-octyl)-resorcinol (7) and 4.25 g (0.05 mol) of piperidine in 30 ml of methanol was heated under reflux for 3 hrs and worked up as described above for the preparation of 2-(α-dimethylaminoacetylaminobenzyl)-5-(3-methyl-2-octyl)-resorcinol hydrochloride (9). There was obtained 1.9 g of (10), mp 195°-198° (from ethanol-ether).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04083868 |
| Source dataset | uspto-grants-1978_04 |
| ORD ID | ord-660c4f3b975e493b848ba4edfb19f942 |
| Source note | uspto-grants-1978_04 |