HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Aminopentan-1-ol → HCID 20300316, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Aminopentan-1-ol | HCID 75634 | — |
| Reactant | 1,1-Bis(methylthio)-2-nitroethylene | HCID 83623 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20300316 | HCID 20300316 | — |
Reaction Steps
Heating 1-nitro-2,2-bis(methylthio)ethylene with an excess of 5-aminopentan-1-ol in ethanol gives 1,1-bis(5-hydroxypentyl)-2-nitroethylene, which may be treated with p-toluenesulphonyl chloride in pyridine and the product heated with thiourea in acetone to give 1,1-bis(5-(S-isothioureido)pentyl)-2-nitroethylene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04084001 |
| Source dataset | uspto-grants-1978_04 |
| ORD ID | ord-bb52a051936943698a9c61544429c4c9 |
| Source note | uspto-grants-1978_04 |