Ethylenediamine → HCID 21332377, compound

HRID 2083345Notes

Reaction equation

HRID 2083345 reaction equation
[CH2:1]1[O:11][CH:2]1[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].[CH2:12]([NH2:15])[CH2:13][NH2:14]>C(O)C>[CH2:12]([NH:15][CH2:1][CH:2]([OH:11])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10])[CH2:13][NH:14][CH2:1][CH:2]([OH:11])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10]

Participants

4

Reactant 2

HCID 3301EthylenediamineHCID 169931,2-Epoxydecane

Product 1

HCID 21332377HCID 21332377, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

In a manner similar to that of Example 1, condensation of 1-decene oxide (100 g.) and ethylenediamine (19.2 g.) and recrystallization of a portion (20 g.) of the resulting solid (45 g.) from ethanol gave N,N'-ethylenebis[2-hydroxydecylamine] (I: R = CH3 (CH2)7, R' = H, X = (CH2)2, Z = H) (13.6 g., m.p. 140.0°-145.8° C.).

Sources & evidence

ORD record
ord-4ec32c0604b349daa97aacd4542909c2
Source dataset
uspto-grants-1978_04
Patent number
US04085144

Reaction notes

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