HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylenediamine → HCID 21332458, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylenediamine | HCID 3301 | — |
| Reactant | 1,2-Epoxydodecane | HCID 17858 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21332458 | HCID 21332458 | — |
Reaction Steps
In a manner similar to that of Example 1, condensation of 1-dodecene oxide (100 g.) and ethylenediamine (16.3 g.) and recrystallization of part (20 g.) of the resulting product (55.3 g.) from methanol gave N,N'-ethylenebis[2-hydroxydodecylamine] (I: R = CH3 (CH2)9, R' = H, X = (CH2)2, Z = H) (13.4 g., m.p. 137.0°-142.0° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04085144 |
| Source dataset | uspto-grants-1978_04 |
| ORD ID | ord-4f31a5485f00414799e19305b08ba466 |
| Source note | uspto-grants-1978_04 |