1,8-Octanediamine → HCID 21332399, compound

HRID 2083356Notes

Reaction equation

HRID 2083356 reaction equation
[CH2:1]1[O:8][CH:2]1[CH2:3][CH2:4][CH2:5][CH2:6][CH3:7].[CH2:9]([NH2:18])[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][NH2:17]>CO>[CH2:9]([NH:18][CH2:1][CH:2]([OH:8])[CH2:3][CH2:4][CH2:5][CH2:6][CH3:7])[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][NH:17][CH2:1][CH:2]([OH:8])[CH2:3][CH2:4][CH2:5][CH2:6][CH3:7]

Participants

4

Reactant 2

HCID 242501,8-OctanediamineHCID 922152-Pentyloxirane

Product 1

HCID 21332399HCID 21332399, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

In a manner similar to that of Example 1, condensation of 1-heptene oxide (52 g.) and 1,8-octanediamine (32.8 g.) and two recrystallizations of the resulting product from methanol gave N,N'-(1,8-octylene)-bis[2-hydroxyheptylamine] (I: R = CH3 (CH2)4, R' = H, X = (CH2)8, Z = H) (17.2 g., m.p. 128.0°-132.8° C.).

Sources & evidence

ORD record
ord-b6a89d9fd58b48e9a7efa8b5fbcffdcd
Source dataset
uspto-grants-1978_04
Patent number
US04085144

Reaction notes

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