HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexanone → 3-Methyl-5,6,7,8-tetrahydroquinoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexanone | HCID 7967 | — |
| Reactant | HCID 3781742 | HCID 3781742 | — |
| Product | 3-Methyl-5,6,7,8-tetrahydroquinoline | HCID 120028 | 30% |
Reaction Steps
The title compound was prepared from commercially available 3-amino-2-methylacrolein and cyclohexanone according to the method of Breitmaier and Bayer (Tet. Letts, 1970, 38, 3291-4) and isolated as a pale yellow oil b.p. 120°/15 mm. (30% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04085215 |
| Source dataset | uspto-grants-1978_04 |
| ORD ID | ord-f6c45ee2c2b44440b864e1624b419e49 |
| Source note | uspto-grants-1978_04 |