HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminum(III) Chloride → 2-Ethyl-2-n-propyl-5-hydroxy-6,7-dichloro-1-indanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | 2-Ethyl-2-n-propyl-5-methoxy-6,7-dichloro-1-indanone | HCID 12395563 | — |
| Solvent | Heptane | HCID 8900 | — |
| Product | 2-Ethyl-2-n-propyl-5-hydroxy-6,7-dichloro-1-indanone | HCID 12395585 | — |
Reaction Steps
2-Ethyl-2-n-propyl-5-hydroxy-6,7-dichloro-1-indanone is prepared following substantially the same procedure described in Example 5, Step F, using the following substances: 2-ethyl-2-n-propyl-5-methoxy-6,7-dichloro-1-indanone (11 g., .037 mole), aluminum chloride (12.5 g., 0.094 mole) and heptane (400 ml.). The above procedure gives 9.0 g. of 2-ethyl-2-n-propyl-5-hydroxy-6,7-dichloro-1-indanone which after recrystallization from methylcyclohexane melts at 153° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04085219 |
| Source dataset | uspto-grants-1978_04 |
| ORD ID | ord-28c1086691214403b992f4ac7a8c6258 |
| Source note | uspto-grants-1978_04 |