HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl bromide → HCID 12395567, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | 1,2-Dimethoxyethane | HCID 8071 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 2-Methyl-5-methoxy-6,7-dichloro-1-indanone | HCID 12395561 | — |
| Product | HCID 12395567 | HCID 12395567 | — |
Reaction Steps
2-Allyl-2-methyl-5-methoxy-6,7-dichloro-1-indanone is prepared following substantially the same procedure described in Example 5, Step E, using the following substances: 2-methyl-5-methoxy-6,7-dichloro-1-indanone (14.7 g., 0.06 mole), sodium hydride (1.7 g., 0.072 mole), 1,2-dimethoxyethane (500 ml.) and allyl bromide (8 ml.). The above procedure gives 11.0 g. of 2-allyl-2-methyl-5-methoxy-6,7-dichloro-1-indanone which after recrystallization from methyl cyclohexane melts at 58° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04085219 |
| Source dataset | uspto-grants-1978_04 |
| ORD ID | ord-1bc2e85b308c4b539ac4d063df665d2e |
| Source note | uspto-grants-1978_04 |