HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2,3-Dichloroanisole → 2',3'-Dichloro-4'-methoxy-2-methylbutyrophenone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2,3-Dichloroanisole | HCID 16126 | — |
| Edukt | Butanoyl chloride, 2-methyl- | HCID 93697 | — |
| Edukt | Aluminum(III) Chloride | HCID 6451240 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | 2',3'-Dichloro-4'-methoxy-2-methylbutyrophenone | HCID 20358455 | — |
Reaktionsschritte
By following the procedure described in Example 5, Step A, using as the reactants 2,3-dichloroanisole (100 g., 0.565 mole), 2-methylbutyryl chloride (.75 g., 0.62 mole), aluminum chloride (83 g., 0.62 mole) and methylene chloride (400 ml.), there is obtained 2',3'-dichloro-4'-methoxy-2-methylbutyrophenone.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04085219 |
| Quelldatensatz | uspto-grants-1978_04 |
| ORD ID | ord-4ddfba3ef775452f9771f1e0fbc49337 |
| Quellennotiz | uspto-grants-1978_04 |