Hydrochloric Acid → HCID 20300394, compound

Participants

Reaction Steps

A slurry of 1.5 g of 4-chloro-1-cyclohexylbenzotriazole, 15 g of sodium methoxide, 10 g of cuprous iodide in 50 ml of 2,4,6-trimethyl pyridine (collidine) and 10 ml of methanol was heated at the reflux temperature for 26 hours. The reaction was cooled and poured into 150 ml of 10% hydrochloric acid. The product was extracted with ethyl ether and on evaporation of the solvent, 0.5 g of an oil was obtained which solidified on standing. The product had a melting point of 133°-134°.

Provenance & Evidence