HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → 1,4-Bis(beta-carboxyethylamino)-2,3-dichloroanthraquinone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Acrylic Acid | HCID 6581 | — |
| Reactant | Boric Acid | HCID 7628 | — |
| Reactant | Disperse Violet 28 | HCID 65731 | — |
| Product | 1,4-Bis(beta-carboxyethylamino)-2,3-dichloroanthraquinone | HCID 20357178 | 93% |
Reaction Steps
20 Parts of acrylic acid are gradually added to a mixture of 15.8 parts of 1,4-diamino-2,3-dichloroanthraquinone, 3.1 parts of boric acid and 100 parts of 100% sulphuric acid at 25°-30° C, and the mixture is then stirred for 60 hours at 25°-30°. The reaction mixture is then processed as described in Example 1 to give 21 parts (93%) of 1,4-bis(β-carboxyethylamino)-2,3-dichloroanthraquinone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04086252 |
| Source dataset | uspto-grants-1978_04 |
| ORD ID | ord-eaf81ab889814be5b9def043bf21ff95 |
| Source note | uspto-grants-1978_04 |