huagongshe.com
HRID2083771

反应详情

EQUATION

反应方程式

HRID 2083771 的结构方程式

REACTANTS

反应物

3
结构：CCC(=O)O
HCID1032

未命名化合物

结构：O=C(OC(=O)c1ccccc1S(=O)(=O)O)c1ccccc1S(=O)(=O)O
HCID13795534

未命名化合物

结构：CN1CCC(C2(O)c3ccc(F)cc3Sc3ccc(F)cc32)CC1
HCID20357479

2,6-Difluoro-9-(1-methylpiperidin-4-yl)-9H-thioxanthen-9-ol

C19H19F2NOS

PRODUCTS

生成物

1
结构：CN1CCC(=C2c3ccc(F)cc3Sc3ccc(F)cc32)CC1
HCID20357530

4-(2,6-Difluoro-9H-thioxanthen-9-ylidene)-1-methylpiperidine

C19H17F2NS

PROCEDURE

实验过程

The thioxanthene-9-ol (2.6 g., 0.0075 mol) prepared as above is heated with 2.8 g. (0.015 mol) of o-sulfobenzoic anhydride in 80 ml. of propionic acid. The product is isolated by the usual procedure to give 4-(2,6-difluoro-9-thioxanthenylidene)-1-methylpiperidine, m.p. 120°-123° C.

WORKUP

后处理

  1. temperatureabove is heated with 2.8 g
  2. customThe product is isolated by the usual procedure