HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2083844Generated: November 2, 2026
Terephthalaldehyde → HCID 69887961, compound
https://huagongshe.com/reaction/2083844
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Terephthalaldehyde | HCID 12173 | — |
| Reactant | (2-Cyanoethyl)hydrazine | HCID 136177 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 69887961 | HCID 69887961 | — |
Reaction Steps
To a suspension of 102 g terephthaldehyde in 700 ml methanol 129.4 g of 2-cyanoethylhydrazine are added drop-wise within 20 minutes. The temperature increases to about 50° C., and an orange-red solution generally arises. After about 10 minutes further crystallization occurs. Stirring continues for 30 minutes and a precipitate that appears is filtered with suction. After washing with a little cold methanol the precipitate is dried under vacuum. 187 g of beige colored product are produced.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06716257B2 |
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| Source dataset | uspto-grants-2004_04 |
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| ORD ID | ord-36cbbf916d1542eab4aa0b916cc6c6eb |
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| Source note | uspto-grants-2004_04 |
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