HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Iodide → HCID 13008376, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Benzene, 1,3-bis(bromomethyl)- | HCID 69373 | — |
| Reactant | 3,5-Dibromo-4-nitro-1H-pyrazole | HCID 13707994 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 13008376 | HCID 13008376 | — |
Reaction Steps
13.54 g of 3,5-dibromo-4-nitropyrazole, 11.1 g potassium carbonate, 0.8 g of potassium iodide and 6.6 g α, α′-dibromo-m-xylene are heated to 100° C. in 40 ml of dimethyl formamide. After 50 minutes the reaction mixture is allowed to cool and poured into 400 ml water. The precipitate is filtered, washed with water and dried in vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06716257B2 |
| Source dataset | uspto-grants-2004_04 |
| ORD ID | ord-fae890e73e584ea99a96392548b8c5fb |
| Source note | uspto-grants-2004_04 |