Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | [4-(4-Chlorophenoxy)phenyl]acetic acid | HCID 15790503 | — |
| Product | HCID 12531835 | HCID 12531835 | — |
Reaction Steps
5.1 g of the product from step C are dissolved in methanol (50 ml). The solution is cooled to −10° C. and treated with thionyl chloride (3 ml) and subsequently heated under reflux for 1 hour. The reaction mixture is evaporated and the residue dissolved in ether. The ether phase is washed with water, dried and evaporated to yield 5.1 g of a reddish brown oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06716845B2 |
|---|
| Source dataset | uspto-grants-2004_04 |
|---|
| ORD ID | ord-3dcaf63de126495fb799f59d44baaeff |
|---|
| Source note | uspto-grants-2004_04 |
|---|
