Benzyl Alcohol → HCID 69891250, compound

Participants

Reaction Conditions

Reaction Steps

To 10 mmol of chlorosulphonyl isocyanate dissolved in dichloromethane at 0° C. there are added, dropwise at 0° C., 10 mmol of benzyl alcohol dissolved in dichloromethane and then, after stirring for 1 hour 30 minutes at 0° C., 10 mmol of the compound obtained in Step B of Example 3, dissolved in a mixture of dichloromethane and triethylamine 96/4. After returning to ambient temperature, the reaction mixture is stirred overnight and then separated. The organic phase is washed, dried and evaporated to yield the expected product.

Provenance & Evidence