Diethylamine → HCID 10036272, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of 6-(2-(Methanesulfonyl)ethyl)-indole (107 mg, 0.45 mmol) and diethylamine (0.4 ml) in 2 ml of THF was stirred at 65° C. overnight. The reaction mixture was concentrated in vacuo and passed through a silica gel column, eluting with 2% 2M ammonia/methanol in dichloromethane, to give the title compound, 42 mg (43% yield).

Provenance & Evidence