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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2084073Generated: October 30, 2026

P-Anisidine → HCID 22732454, compound

https://huagongshe.com/reaction/2084073

Reaction equation

Participants

RoleNameHCIDCharge
ReactantP-AnisidineHCID 7732—
Reactant4-chloro-6-methyl-2-(3-methylphenyl)pyrimidineHCID 4189212—
ProductHCID 22732454HCID 22732454—

Reaction Steps

The title compound was prepared from 4-chloro-6-methyl-2-(3-methylphenyl)pyrimidine (100 mg, 0.457 mmol) and p-anisidine (56 mg, 0.457 mmol), similar to Example 11 as a pale green solid (39 mg, 28%). 1H NMR (DMSO-d6): 8.04 (s, 1H), 8.01-7.99 (m, 1H), 7.56-7.51 (m, 4H), 7.04 (d, J=9.0 Hz, 2H), 6.73 (s, 1H), 3.79 (s, 3H), 2.44 (s, 6H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06716851B2
Source datasetuspto-grants-2004_04
ORD IDord-93b8c2c0ad0643768972fb0b0089fa6f
Source noteuspto-grants-2004_04