HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxyaniline → HCID 22732501, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxyaniline | HCID 10824 | — |
| Reactant | 4-CHLORO-5-METHOXY-2-(2-PYRIDINYL)PYRIMIDINE | HCID 2763500 | — |
| Product | HCID 22732501 | HCID 22732501 | — |
Reaction Steps
The title compound was prepared from 4-chloro-5-methoxy-2-(2-pyridinyl)pyrimidine (100 mg, 0.451 mmol) and m-anisidine (51 μl, 0.451 mmol) similar to Example 13 and isolated as a tan oily liquid (63 mg, 45%). 1H NMR (CDCl3): 8.76-8.74 (m, 1H), 8.37 (dd, J=1.1, 8.0 Hz, 1H), 8.05 (s, 1H), 7.79-7.73 (m, 2H), 6.65-6.62 (m, 1H), 3.92 (s, 3H), 3.84 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06716851B2 |
| Source dataset | uspto-grants-2004_04 |
| ORD ID | ord-fcf4a7ba27404fce9011eb15e8a091e2 |
| Source note | uspto-grants-2004_04 |