HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Aminobenzonitrile → HCID 22732384, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Aminobenzonitrile | HCID 16702 | — |
| Reactant | 4-Chloro-6-methyl-2-(pyridin-2-yl)pyrimidine | HCID 2763395 | — |
| Product | HCID 22732384 | HCID 22732384 | — |
Reaction Steps
The title compound was prepared from 4-chloro-6-methyl-2-(2-pyridinyl)pyrimidine (100 mg, 0.486 mmol) and 3-aminobenzonitrile (57 mg, 0.486 mmol) similar to Example 11 and isolated as a pale white solid (107 mg, 76%). 1H NMR (DMSO-d6): 10.14 (s, 1H), 8.78-8.75 (m, 1H), 8.56 (s, 1H), 8.32 (d, J=7.8 Hz, 1H), 8.04-7.96 (m, 2H), 7.60-7.47 (m, 3H), 6.75 (s, 1H) 2.47 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06716851B2 |
| Source dataset | uspto-grants-2004_04 |
| ORD ID | ord-ac685c79830d40bf91b0662de8c100a6 |
| Source note | uspto-grants-2004_04 |