3-Ethylaniline → HCID 22732531, compound

Participants

Reaction Steps

The title compound was prepared from 4-chloro-6-methyl-2-(2-pyridinyl)pyrimidine (50 mg, 0.243 mmol) and 3-ethylaniline (60 μl, 0.243 mmol) similar to Example 13 and isolated as an tan oil (69 mg, 98%). 1H NMR (CDCl3): 8.81-8.79 (m, 1H), 8.48-8.45 (m, 1H), 7.84-7.78 (m, 1H), 7.42 (s, 1H), 7.37-7.29 (m, 2H), 7.18 (s, 1H), 7.16 (d, J=1.5 Hz, 1H), 7.02 (d, J=7.8 Hz, 1H), 6.61 (s, 1H), 2.66 (q, J=7.5 Hz, 2H), 2.47 (s, 3H), 1.25 (t, J=7.5 Hz, 3H).

Provenance & Evidence