HRID2084133

反应详情

EQUATION

反应方程式

HRID 2084133 的结构方程式

PROCEDURE

实验过程

The title compound was prepared from a mixture of 4-chloro-2-phenyl-6-(trifluoromethyl)pyrimidine (50 mg, 0.193 mmol) and 3,4-methylenedioxyaniline (40 mg, 0.290 mmol) similar to Example 77 and isolated as a tan solid (16 mg, 23%). 1H NMR (CDCl3): 8.44-8.40 (m, 2H), 7.50-7.45 (m, 3H), 7.02 (s, 1H), 6.91 (s, 1H), 6.85 (d, J=8.1 Hz, 1H), 6.78 (dd, J=2.0, 8.3 Hz, 1H), 6.71 (s, 1H), 6.03 (s, 2H).