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3-(Trifluoromethyl)benzaldehyde → 3,4,5-trimethoxy-N'-{[3-(trifluoromethyl)phenyl]methylidene}benzohydrazide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-(Trifluoromethyl)benzaldehyde | HCID 67990 | — |
| 反応物 | 3,4,5-Trimethoxybenzohydrazide | HCID 76793 | — |
| 生成物 | 3,4,5-trimethoxy-N'-{[3-(trifluoromethyl)phenyl]methylidene}benzohydrazide | HCID 2399573 | — |
反応手順
The title compound was prepared from 3,4,5-trimethoxy-benzoic acid hydrazide and 3-trifluoromethyl-benzaldehyde by a procedure similar to Example 22. 1H NMR (DMSO-d6): 11.93 (s, 1H), 8.57 (s, 1H), 8.08 (s, 1H), 8.05 (d, J=8.1 Hz, 1H), 7.82 (d, J=7.5 Hz, 1H), 7.74 (d, J=7.5 Hz, 1H), 7.26 (s, 2H), 3.89 (s, 6H), 3.75 (s, 3H). MS (MH+, MH−): 451, 453.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06716859B2 |
| 出典データセット | uspto-grants-2004_04 |
| ORD ID | ord-70eaed4c2d344232b68c55f2bc3108e9 |
| 出典メモ | uspto-grants-2004_04 |