HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 69829492, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Aminoacetaldehyde dimethyl acetal | HCID 89728 | — |
| Reactant | HCID 15965801 | HCID 15965801 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 69829492 | HCID 69829492 | 28.1% |
Reaction Steps
Using (3S)-4-(benzyloxy)-3-hydroxybutyronitrile (6.51 g), a 5.12 N solution of hydrogen chloride in ether (7.0 ml), and aminoacetaldehyde dimethyl acetal (3.58 g), the same reaction as Reference Example 6 was carried out to yield the titled compound (2.22 g) as a light-brown oily substance.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06716863B2 |
| Source dataset | uspto-grants-2004_04 |
| ORD ID | ord-5d8bbdf7a05b42eabaaecf418ca3db77 |
| Source note | uspto-grants-2004_04 |