HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54204380, compound → 4-(4-Hydroxybutyl)phenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54204380 | HCID 54204380 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | MeOH tetrahydrofuran | HCID 21899815 | — |
| Product | 4-(4-Hydroxybutyl)phenol | HCID 13392513 | 99% |
Reaction Steps
4-(4-benzyloxyphenyl)-3-buten-1-ol (1.70 g) was dissolved in a mixture of methanol-THF (1:1, 20 ml); 10% palladium carbon (0.17 g) was added, followed by vigorous stirring in a hydrogen atmosphere for 1.5 hours. The catalyst was filtered off; the filtrate was concentrated under reduced pressure to yield the titled compound (1.1 g) as a colorless crystalline powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06716863B2 |
| Source dataset | uspto-grants-2004_04 |
| ORD ID | ord-607b9c6a9c9f4b3f96dfa5dff74ca933 |
| Source note | uspto-grants-2004_04 |