HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-[4-(4-benzyloxyphenyl)butyl)-1H-1,2,3-triazole → 4-(4-[1,2,3]Triazol-1-yl-butyl)phenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-[4-(4-benzyloxyphenyl)butyl)-1H-1,2,3-triazole | HCID 22733349 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 4-(4-[1,2,3]Triazol-1-yl-butyl)phenol | HCID 12109494 | 99.8% |
Reaction Steps
1-[4-(4-benzyloxyphenyl)butyl]-1H-1,2,3-triazole (0.38 g) was dissolved in methanol (7.6 ml); 10% palladium carbon (0.1 g) was added, followed by vigorous stirring in a hydrogen atmosphere for 14 hours. The catalyst was filtered off; the filtrate was concentrated to dryness under reduced pressure to yield the titled compound (0.268 g) as a crystalline powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06716863B2 |
| Source dataset | uspto-grants-2004_04 |
| ORD ID | ord-1e898b3b8cd242da9b7bcf2cb7f72955 |
| Source note | uspto-grants-2004_04 |