Carbamic chloride, N-methyl-N-phenyl- → HCID 22397362, compound

HRID 2084671Notes

Reaction equation

HRID 2084671 reaction equation
[CH3:1][N:2]([C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1)[C:3](Cl)=[O:4].[NH2:12][CH2:13][CH2:14][CH2:15][N:16]1[C:24]2[C:23]([CH3:25])=[C:22]([CH3:26])[N:21]=[C:20]([NH2:27])[C:19]=2[N:18]=[C:17]1[CH2:28][O:29][CH2:30][CH3:31]>>[NH2:27][C:20]1[C:19]2[N:18]=[C:17]([CH2:28][O:29][CH2:30][CH3:31])[N:16]([CH2:15][CH2:14][CH2:13][NH:12][C:3](=[O:4])[N:2]([CH3:1])[C:6]3[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=3)[C:24]=2[C:23]([CH3:25])=[C:22]([CH3:26])[N:21]=1

Participants

3

Reactant 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 219738361-(3-aminopropyl)-2-(ethoxymethyl)-6,7-dimethyl-1H-imidazo[4,5-c]pyridin-4-amine

Product 1

HCID 22397362HCID 22397362, compound

Procedure

Using the method of Examples 94-105, N-methyl-N-phenylcarbamoyl chloride was reacted with 1-(3-aminopropyl)-2-(ethoxymethyl)-6,7-dimethyl-1H-imidazo[4,5-c]pyridin-4-amine to provide the desired compound. The observed accurate mass was 411.2513.

Sources & evidence

ORD record
ord-27c1a0efb1a34ba692348ef6f4ad4d04
Source dataset
uspto-grants-2004_04
Patent number
US06716988B2

Reaction notes

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