2-Phenylethanol → HCID 22734399, compound

HRID 2084785Notes

Reaction equation

HRID 2084785 reaction equation
[C:1]([CH2:4][C:5]1[C:9]2[C:10]([C:16](=[O:26])[CH2:17][C:18]3[C:23]([Cl:24])=[CH:22][N:21]=[CH:20][C:19]=3[Cl:25])=[CH:11][CH:12]=[C:13]([O:14][CH3:15])[C:8]=2[O:7][CH:6]=1)([OH:3])=[O:2].[CH2:27](O)[CH2:28][C:29]1[CH:34]=[CH:33][CH:32]=[CH:31][CH:30]=1>>[Cl:24][C:23]1[CH:22]=[N:21][CH:20]=[C:19]([Cl:25])[C:18]=1[CH2:17][C:16]([C:10]1[C:9]2[C:5]([CH2:4][C:1]([O:3][CH2:27][CH2:28][C:29]3[CH:34]=[CH:33][CH:32]=[CH:31][CH:30]=3)=[O:2])=[CH:6][O:7][C:8]=2[C:13]([O:14][CH3:15])=[CH:12][CH:11]=1)=[O:26]

Participants

3

Reactant 2

HCID 60542-PhenylethanolHCID 22733964HCID 22733964, compound

Product 1

HCID 22734399HCID 22734399, compoundYield 36%

Procedure

Substantially the same procedure as in Example 13 was repeated using Compound 151 (0.30 g) obtained in Example 151 and phenethyl alcohol (0.7 ml) to give Compound 153 (0.14 g, 36%) as white crystals.

Sources & evidence

ORD record
ord-da01a708e47f424896a42f14ae6dd859
Source dataset
uspto-grants-2004_04
Patent number
US06716987B1

Reaction notes

Loading…