Sodium Iodide → HCID 69804715, compound

Participants

Reaction Steps

To a solution of 0.910 g (0.2.619 mmol) of the product of Example 44 in 30 mL of DMF was added 0.432 g (0.2.881 mmol) of sodium iodide. The reaction was stirred for 30 min at room temperature and then 0.590 mL (5.499 mmol) of benzylamine and 0.96 mL (5.499 mmol) of diisopropylethylamine was added and the resulting mixture was heated at 80 degrees for 3 h and then cooled to room temperature.

Provenance & Evidence