HuagongsheHuagongshe Chemistry Print Report · For research reference only
4,6-Dichloro-5-(2-methoxyphenoxy)-2,2'-bipyrimidine → 4-Tert-butyl-n-(6-chloro-5-(2-methoxyphenoxy)-2,2'-bipyrimidin-4-yl)benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4,6-Dichloro-5-(2-methoxyphenoxy)-2,2'-bipyrimidine | HCID 10545706 | — |
| Reactant | HCID 131721323 | HCID 131721323 | — |
| Product | 4-Tert-butyl-n-(6-chloro-5-(2-methoxyphenoxy)-2,2'-bipyrimidin-4-yl)benzenesulfonamide | HCID 11135160 | — |
Reaction Steps
4-tert.-butyl-N-[6-chloro-5-(o-methoxyphenoxy)-2-(2-pyrimidinyl)-4-pyrimidinyl]benzene sulfonamide was prepared as disclosed in EP 0 526 708 A1 from 4,6-dichloro-5-(o-methoxyphenoxy)-2-(2-pyrimidinyl)-pyrimidine and p-tert.-butyl benzene sulfonamide potassium salt. LC-MS: tR=5.50 min, [M+1]+=526.29, [M−1]−=524.43.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06720322B2 |
| Source dataset | uspto-grants-2004_04 |
| ORD ID | ord-5889c480d3774eeab3261013243a4429 |
| Source note | uspto-grants-2004_04 |