HuagongsheHuagongshe Chemistry Print Report · For research reference only
7-Methoxybenzofuran-2-carbonitrile → 1-(Hydroxyimino)-1-(7-methoxybenzo(b)furan-2-yl)methylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 7-Methoxybenzofuran-2-carbonitrile | HCID 298556 | — |
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Product | 1-(Hydroxyimino)-1-(7-methoxybenzo(b)furan-2-yl)methylamine | HCID 3069470 | 92.4% |
Reaction Steps
By the reactions in the same manner as in Starting Material Synthesis Example 28 using 7-methoxybenzo(b)furan-2-carbonitrile (3.0 g), hydroxylamine hydrochloride (1.4 g) and sodium hydrogencarbonate (2.1 g), the title compound (3.3 g) was obtained as brown crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06720320B2 |
| Source dataset | uspto-grants-2004_04 |
| ORD ID | ord-7921f5c995394533b9ba8a1a8fdf7c97 |
| Source note | uspto-grants-2004_04 |