HuagongsheHuagongshe Chemistry Print Report · For research reference only
(S)-(+)-Glycidyl-4-nitrobenzoate → (s)-3-(7-Glycidyloxybenzo(b)furan-2-yl)-5-methyl-1,2,4-oxadiazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (S)-(+)-Glycidyl-4-nitrobenzoate | HCID 10868995 | — |
| Reactant | 3-(7-Hydroxybenzo(b)furan-2-yl)-5-methyl-1,2,4-oxadiazole | HCID 22729084 | — |
| Product | (s)-3-(7-Glycidyloxybenzo(b)furan-2-yl)-5-methyl-1,2,4-oxadiazole | HCID 60078028 | 90% |
Reaction Steps
By the reactions in the same manner as in Starting Material Synthesis Example 1 using 3-(7-hydroxybenzo(b)furan-2-yl)-5-methyl-1,2,4-oxadiazole (1.5 g) and (S)-glycidyl nosylate (1.8 g), the title compound (1.7 g) was obtained as white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06720320B2 |
| Source dataset | uspto-grants-2004_04 |
| ORD ID | ord-58383f3288c644b3b50ca9e2ee80b294 |
| Source note | uspto-grants-2004_04 |