HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → (s)-5-(4-Glycidyloxybenzo(b)furan-2-yl)-3-methylisoxazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | (S)-(+)-Glycidyl-4-nitrobenzoate | HCID 10868995 | — |
| Reactant | HCID 135794328 | HCID 135794328 | — |
| Product | (s)-5-(4-Glycidyloxybenzo(b)furan-2-yl)-3-methylisoxazole | HCID 60077892 | 86.3% |
Reaction Steps
By the reactions in the same manner as in Starting Material Synthesis Example 1 using 5-(4-hydroxybenzo(b)furan-2-yl)-3-methylisoxazole (2.6 g), (S)-glycidyl nosylate (3.1 g) and potassium carbonate (5.0 g), the title compound (2.8 g) was obtained as brown crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06720320B2 |
| Source dataset | uspto-grants-2004_04 |
| ORD ID | ord-cb5e14d205f8470ba384ccf03c55ad92 |
| Source note | uspto-grants-2004_04 |