99329-54-1 → HCID 69497907, compound

HRID 2085237Notes

Reaction equation

HRID 2085237 reaction equation
[CH2:1]([O:5][C:6]1[CH:7]=[C:8]([CH:16]=[CH:17][CH:18]=1)[CH:9]=[C:10]1[CH2:15][CH2:14][O:13][C:11]1=[O:12])[C@H:2]1[O:4][CH2:3]1.[Cl:19][C:20]1[CH:21]=[C:22]([CH:27]2[CH2:32][CH2:31][NH:30][CH2:29][CH2:28]2)[CH:23]=[CH:24][C:25]=1[Cl:26]>>[ClH:19].[Cl:19][C:20]1[CH:21]=[C:22]([CH:27]2[CH2:32][CH2:31][N:30]([CH2:3][C@H:2]([OH:4])[CH2:1][O:5][C:6]3[CH:7]=[C:8]([CH:16]=[CH:17][CH:18]=3)[CH:9]=[C:10]3[CH2:15][CH2:14][O:13][C:11]3=[O:12])[CH2:29][CH2:28]2)[CH:23]=[CH:24][C:25]=1[Cl:26]

Participants

3

Reactant 2

HCID 1624427299329-54-1HCID 86585646HCID 86585646, compound

Product 1

HCID 69497907HCID 69497907, compound

Procedure

In the same manner as in Example 425, the title compound was synthesized from (S)-α-(3-glycidyloxybenzylidene)-γ-butyrolactone and 4-(3,4-dichlorophenyl)piperidine, melting point 147-149° C.

Sources & evidence

ORD record
ord-fd5b3175822a4a6fbdf4a809a67a2a3c
Source dataset
uspto-grants-2004_04
Patent number
US06720320B2

Reaction notes

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