Carbamic chloride, N-methyl-N-phenyl- → HCID 22397370, compound

HRID 2085315Notes

Reaction equation

HRID 2085315 reaction equation
[CH3:1][N:2]([C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1)[C:3](Cl)=[O:4].[CH2:12]([O:14][CH2:15][C:16]1[N:17]([CH2:28][CH2:29][CH:30]2[CH2:35][CH2:34][NH:33][CH2:32][CH2:31]2)[C:18]2[C:23]([CH3:24])=[C:22]([CH3:25])[N:21]=[C:20]([NH2:26])[C:19]=2[N:27]=1)[CH3:13]>>[NH2:26][C:20]1[C:19]2[N:27]=[C:16]([CH2:15][O:14][CH2:12][CH3:13])[N:17]([CH2:28][CH2:29][CH:30]3[CH2:35][CH2:34][N:33]([C:3]([N:2]([CH3:1])[C:6]4[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=4)=[O:4])[CH2:32][CH2:31]3)[C:18]=2[C:23]([CH3:24])=[C:22]([CH3:25])[N:21]=1

Participants

3

Reactant 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 129729622-(ethoxymethyl)-6,7-dimethyl-1-(2-piperidin-4-ylethyl)-1H-imidazo[4,5-c]pyridin-4-amine

Product 1

HCID 22397370HCID 22397370, compound

Procedure

Using the method of Examples 54-65, N-methyl-N-phenylcarbamoyl chloride was reacted with 2-(ethoxymethyl)-6,7-dimethyl-1-(2-piperidin-4-ylethyl)-1H-imidazo[4,5-c]pyridin-4-amine to provide the desired compound. The observed accurate mass was 465.3006.

Sources & evidence

ORD record
ord-ea9e06f21b1942eeba9abbd0472f73a2
Source dataset
uspto-grants-2004_04
Patent number
US06720334B2

Reaction notes

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