HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acrylonitrile → HCID 22725172, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acrylonitrile | HCID 7855 | — |
| Reactant | 4-Phenylpiperidine | HCID 69873 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22725172 | HCID 22725172 | 99% |
Reaction Steps
Acrylonitrile (3.1 mL, 44 mmol, 2.5 eq) was added to a solution of 4-phenylpiperidine (3.00 g, 18.0 mmol) in EtOH (40 mL) and the mixture was stirred at room temperature for 1.5 h. The volatiles were removed, giving 3.80 g of the desired product (brown oil, 99%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06720324B2 |
| Source dataset | uspto-grants-2004_04 |
| ORD ID | ord-ef60bc231152492e87b93e553d58ae80 |
| Source note | uspto-grants-2004_04 |