Pentane → HCID 22731326, compound

Participants

Reaction Steps

Following General Procedure A and using 5-bromo-3,3-dimethyl-7-(2,2-dimethyl-propyl)-2,3-dihydro-benzofuran (Intermediate 32, 0.7 g, 2.37 mmol), 15 mL of anhydrous tetrahydrofuran, 1.7M solution of t-butyllithium in n-pentane (3.53 mL, 6 mmol) and trimethyl borate (0.75 mL, 6 mmol) the title compound was obtained as a foam that was used as such for the next step without purification and characterization.

Provenance & Evidence