HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pentane → 2-Heptyl-phenylboronic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pentane | HCID 8003 | — |
| Reactant | Trimethyl borate | HCID 8470 | — |
| Reactant | 1-Bromo-2-heptyl-benzene | HCID 22731318 | — |
| Reactant | HCID 178418306 | HCID 178418306 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 2-Heptyl-phenylboronic acid | HCID 22731351 | — |
Reaction Steps
Following General Procedure A and using 1-bromo-2-heptyl-benzene (Intermediate 67, 0.4 g, 1.56 mmol), 4 mL of anhydrous tetrahydrofuran, 1.7M solution of t-butyllithium in n-pentane (1.84 mL, 3.1 mmol) and trimethyl borate (0.45 mL, 3.1 mmol), the title compound was obtained (0.27 g, 50%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06720423B2 |
| Source dataset | uspto-grants-2004_04 |
| ORD ID | ord-26709f5f3ae0464cba4168e307ab99a6 |
| Source note | uspto-grants-2004_04 |