Ethanol → HCID 10341969, compound

Participants

Reaction Steps

Following General Procedure H and using (E)-3-((E)-2-{(1S, 2S)-2-[7-(4-methoxy-phenyl)-3,3-dimethyl-2,3-dihydro-benzofuran-5-yl]-2-methyl-cyclopropyl}-vinyl)-but-2-enoic acid ethyl ester (Compound 31, 0.041 g, 0.09 mmol), ethanol (5 mL), and 5M aqueous sodium hydroxide followed by preparative reverse phase HPLC using 10% water in acetonitrile as the mobile phase, the title compound was obtained (0.026 g, 65%).

Provenance & Evidence