Dichloromethane → HCID 10253349, compound

Participants

Reaction Steps

Following General Procedure F and using (E)-3-((E)-2-{(1S,2S)-2-[7-(3-hydroxy-heptyl)-3,3-dimethyl-2,3-dihydro-benzofuran-5-yl]-2-methyl-cyclopropyl}-vinyl)-but-2-enoic acid ethyl ester (Compound 38, 0.019 g, 0.042 mmol), dichloromethane (2.5 mL), acetonitrile (0.5 mL), 4A° molecular sieves powder (0.15 g), tetra-n-propylammoniumperruthenate (0.012 g) and N-methylmorpholine-N-oxide (0.07 g, 0.6 mmol), the title compound was obtained (0.012 g, 58%).

Provenance & Evidence