HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-BOC-ethylenediamine → HCID 131724406, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-BOC-ethylenediamine | HCID 187201 | — |
| Reactant | 2-Chloro-5-(2-chloroethyl)amino-N-(tricyclo[3.3.1.13,7]dec-1-ylmethyl)benzamide | HCID 11417653 | — |
| Product | HCID 131724406 | HCID 131724406 | 94.4% |
Reaction Steps
Prepared according to the method of Example 4 using 2-chloro-5-(2-chloroethyl)amino-N-(tricyclo[3.3.1.13,7]dec-1-ylmethyl)-benzamide (WO 99/29661) (0.2 g) and (2-amino-ethyl)-carbamic acid tert butyl ester (0.25 g) to deliver the sub-title compound as a brown oil (0.25 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06720452B2 |
| Source dataset | uspto-grants-2004_04 |
| ORD ID | ord-42e6d5facb4b46d9bd8b43d0df5a622a |
| Source note | uspto-grants-2004_04 |