HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68452905, compound → HCID 68455470, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68452905 | HCID 68452905 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 68455470 | HCID 68455470 | — |
Reaction Steps
A mixture of Example 126B in TFA (20 mL) and dichloromethane (20 mL) at room temperature was stirred for 1 hour and concentrated to provide the desired product. MS (ESI (+)) m/e 721 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06720338B2 |
| Source dataset | uspto-grants-2004_04 |
| ORD ID | ord-573bbcb336f44dbdb0a65f86666d9f76 |
| Source note | uspto-grants-2004_04 |