Dipropylamine → HCID 9946468, compound

Participants

Reaction Steps

Prepared from the compound of Example 2 and dipropylamine. To a solution of 2-chloro-N-(5,6-dihydro-6-oxo-2-phenanthridinyl-acetamide (45 mg) in N,N-dimethylformamide (10 mL) was added potassium phosphate (68 mg) and dipropylamine (0.027 mL). The solution stirred at room temperature for 5 hours followed by evaporation of the solvent. The light brown product was washed with water and filtered (25 mg). 1H-NMR (300 MHz, DMSO-d6), 11.70 (br s, 1H), 9.72 (br s, 1H), 8.33 (d, J=8.0 Hz, 2H), 7.89 (m, 1), 7.66 (m, 2H), 7.33 (m, 1H), 3.21 (s, 2H), 1.50 (m, 6H), 0.89 (m, 8H).

Provenance & Evidence