Diethyl Ether → HCID 22493753, compound
Reaction equation
[CH2:1]([N:5]1[C:9]([CH:10]=[O:11])=[CH:8][N:7]=[C:6]1[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1)[CH2:2][CH2:3][CH3:4].[CH2:18](OCC)C>>[CH2:1]([N:5]1[C:9]([CH:10]([OH:11])[CH3:18])=[CH:8][N:7]=[C:6]1[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1)[CH2:2][CH2:3][CH3:4]Participants
3
Procedure
A solution of aldehyde 102 (230 mg) in diethyl ether (30 mL) is placed in a separatory funnel and treated with a solution of
Workup
- additiontreated with a solution of
Sources & evidence
- ORD record
- ord-0514c02b21634701a50b83453845250b
- Source dataset
- uspto-grants-2004_04
- Patent number
- US06723743B1
Reaction notes
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